Nolva crashed and crystalized!!!

  1. Question Nolva crashed and crystalized!!!


    WTF. I hvae made this tons of times.

    Used ethyl alcohol 180 proof as main carrier.
    Tamoxifen Citrate 10g
    Peg 400 40ml
    BA 20ml
    BB 20ml

    Heated to make solution 20mg/ml

    After it cooled it crystalized and completely crashed. I know the source is good. Any thoughts??? What would cause that?


  2. usually having to much in relation to the amount of solvent..

  3. Quote Originally Posted by Fayde
    WTF. I hvae made this tons of times.

    Used ethyl alcohol 180 proof as main carrier.
    Tamoxifen Citrate 10g
    Peg 400 40ml
    BA 20ml
    BB 20ml

    Heated to make solution 20mg/ml

    After it cooled it crystalized and completely crashed. I know the source is good. Any thoughts??? What would cause that?
    Not sure but I have had this problem with some of mine. I supect the powder is only 90% or so and that was the problem. I just take mind EOD and reheat as needed (nolva has a long half life, no need to take ED)
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  4. I use PGA only (190 proof) and I get 99% aprox into soln. I really see no point to using so many solvents.

  5. everclear will work fine by itself at 50mg/ml but it will eventually start to crystalize. Even peg won't keep it in solution forever.

  6. Quote Originally Posted by Kitchen Chemist
    everclear will work fine by itself at 50mg/ml but it will eventually start to crystalize. Even peg won't keep it in solution forever.
    Agreed I usually use everclear with no problems. But after it sits for a few weeks without use you can see crystals start to form at the bottom. I just reheat in a pot of boiling water for honestly about a minute and it's all good again. You used a ****load of chems bro and you didn't really need to maybe it had something to do with that. What I might do is take 25mL of the solution add another 25mL of the 180proof and reheat and see if that works. You could also try the same experiment with the peg400. Also when you reheat make sure a cap is on the bottle and let it cool with the cap on. Good luck

  7. I have also found that it tends to crystallize less in Nalgaline containers. It seems to crystallize worse in glass.
  

  
 

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