Question for Syno Guru: Golden Test?

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    Question Question for Syno Guru: Golden Test?


    If someone were to attempt to convert Syno to TNE as shown elsewhere on this board, and it were to turn a bright golden-yellow upon addition of the saturated Sodium hydroxide solution to the methenol syno solution, and produce a final product the same color, is that bad?

    Anyone seen this phenomena? I got the impression everyone got white powder (or crystals).

    Greenguy


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    Quote Originally Posted by candle25
    Thanks, I have read this thread.

    Are you saying that he used too much sodium hydroxide and that if he washes it enough it will be OK?

    I was really hoping for a chemistry type explanation for the golden color, and therefore what its significance was.

    Greenguy

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    Quote Originally Posted by Greenguy
    If someone were to attempt to convert Syno to TNE as shown elsewhere on this board, and it were to turn a bright golden-yellow upon addition of the saturated Sodium hydroxide solution to the methenol syno solution, and produce a final product the same color, is that bad?

    Anyone seen this phenomena? I got the impression everyone got white powder (or crystals).

    Greenguy
    nah, mine was golden in color also, not a problem.

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    The NaOH is used to cleave the estradiol as well as the ester from the test. As for the colormetric change in regards to the NaOH addition, I can't really say what is happening. Maybe Chemo will give some insight into this.

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    Smile


    Quote Originally Posted by jweave23
    nah, mine was golden in color also, not a problem.
    Thanks Jweave, I feel a lot better now!

    Greenguy

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    The color change is due to the products of the saponification reaction. Nothing to worry about as long as it washes out...

    Chemo

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