Question for Syno Guru: Golden Test?

Greenguy

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If someone were to attempt to convert Syno to TNE as shown elsewhere on this board, and it were to turn a bright golden-yellow upon addition of the saturated Sodium hydroxide solution to the methenol syno solution, and produce a final product the same color, is that bad?

Anyone seen this phenomena? I got the impression everyone got white powder (or crystals).

Greenguy
 

jweave23

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If someone were to attempt to convert Syno to TNE as shown elsewhere on this board, and it were to turn a bright golden-yellow upon addition of the saturated Sodium hydroxide solution to the methenol syno solution, and produce a final product the same color, is that bad?

Anyone seen this phenomena? I got the impression everyone got white powder (or crystals).

Greenguy
nah, mine was golden in color also, not a problem. :)
 
candle25

candle25

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The NaOH is used to cleave the estradiol as well as the ester from the test. As for the colormetric change in regards to the NaOH addition, I can't really say what is happening. Maybe Chemo will give some insight into this.
 
Chemo

Chemo

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The color change is due to the products of the saponification reaction. Nothing to worry about as long as it washes out...

Chemo
 
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